During this reporting period START continued to hazcat unknown materials, while ERRS continued to overpack 55-gallon drums and continued to consolidate the materials in each waste stream. An EPA-EPM and EPA-CI were also on-site reviewing historical files and office paper work.
To date, 302 55-gallon containers, 175 small containers, 29 ASTs, and 6 miscellaneous items, have been sampled and categorized by onsite hazcat testing. The 55-gallon drums and small containers have been consolidated into 281 55-gallon containers and/or 85-gallon overpacks. The 281 drums are currently subdivided into 5 waste streams: 149 non-haz, 66 bases, 47 chlorides, 17 acids, and 2 flammables waste drums. In addition, 374 items in the chemical laboratory closet have been cataloged.
ERRS worked on reconditioning the base valves of each onsite AST. Rusted and closed valves were and reopened and where necessary, piping was added/adapted to accommodate for the pumping of the tank contents when needed.
In preparation for disposal, companies were contacted as part of the RFQ for the material inside ASTs 1, 2, and 3. All companies requested a composite sample of the material in the tanks. On October 26 the three tanks were sampled (bitters- not bottoms) and an aliquot of the composite sample were sent to each bidder that requested samples. On October 27 all the bidders reported that the material had no glycol products. Upon request, on October 27, a second composite sample from each of the three tanks (bottom – heavier constituents below bitters) was sent to two of the initial bidders that requested samples. The second sample was taken from the lowest part of the tank. The bidders felt that if there were glycol compounds in the tank that they would be found at the bottom of the tank due to glycol having a higher specific gravity than water. On October 28, it was reported that no glycol compounds were in the samples taken from the bottom of the tank either. These results have led the bidders to request a BTU test on the materials.
The results for the asbestos sampling event arrived on October 25, 2010. All materials tested resulted in non-detect for chrysotile, amosite, crocidolite, actinolite, tremolite, or anthophylite. No asbestos was found around the glycol recycler. There was no other evidence of asbestos containing material onsite.